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Correlation between the calcination and sintering temperature on phase formation, microstructure and dielectric properties of SrTiO3 ceramics
Abdelhalim Elbasset1, Tajddin. Lamcharfi2, Farid Abdi3, Hicham Laribou4, Abdelhak Elghandouri5, Lamiae Mrharrab6.
The aim of this work is to investigate the effect of calcination temperature (600, 700 and
800°C) and sintering temperature (1000, 1050 and 1100°C) on pure phase formation,
microstructure and dielectric properties of perovskite SrTiO3 (ST) ceramics. The results
show that the calcination conditions at 600°C for 6h, are sufficient to obtain this phase.
Furthermore, lattice parameter (a) tends to increase with increasing calcinations
temperature. The Raman spectroscopy characterization indicates the presence in the
calcination spectrum at 600°C of extra-modes located around 113 and 617 cm-1. The optical
absorption edge of SrTiO3 was explored in the temperature from 200 to 1000°C. The results
suggest that the band gap energy is increasing with temperature. On the other hand, the
results found show that the average grain size of the sintered ST at 1100°C is the order of
12µm which is respectively larger than that at 1000 (~ 3.2µm) and at 1050°C (~ 6.4µm). The
dielectric study shows that samples sintered at 1100°C have smaller and stable dielectric
losses as a function of frequency
Affiliation:
- University Sidi Mohamed ben Abdellah, Fez, Morocco
- University Sidi Mohamed ben Abdellah, Fez, Morocco
- University Sidi Mohamed ben Abdellah, Fez, Morocco
- University of Lorraine, France
- FSDM B.P. 179, Fez. , Morocco
- FSDM B.P. 179, Fez. , Morocco
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Indexation |
Indexed by |
MyJurnal (2021) |
H-Index
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2 |
Immediacy Index
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0.000 |
Rank |
0 |
Indexed by |
Scopus 2020 |
Impact Factor
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CiteScore (1.3) |
Rank |
Q3 (Electrical and Electronic Engineering)) Q4 (Electronic, Optical and Magnetic Materials) |
Additional Information |
SJR (0.298) |
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