The liquid level control in tanks and flow control between cascaded or coupled tanks are the basic control problems exist in process industries nowadays. Liquids are to be pumped, stored or mixed in tanks for various types of chemical processes and all these require essential control and regulation of flow and liquid level. In this paper, different types of tuning methods are proposed for Proportional-Integral (PI) controller and are further improved with integration of Advanced Process Control (APC) method such as feedforward and gain scheduling to essentially control the liquid level in Tank 2 of a coupled tank system. The MATLAB/Simulink tools are used to design PI controller using pole-placement, Ciancone, Cohen Coon and modified Ziegler-Nichols tuning method with Cohen Coon tuning method found to have a better performance. Advanced process control such as feedforward-plus-PI, Gain Scheduling (GS) based PI, Internal Model Control (IMC) based PI, feedforward-plus-GS-based PI and feedforward-plus-IMCbased PI controllers are further tested as improvement version to further compare the significance of the advanced process control outcomes hence GS-PI, improved GI-base PI-plus FF found to have better performance. The GS method is built over five operating points to approximate the system’s nonlinearity and is eventually combined with feedforward control to yield a much better performance.